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Rapid Method for Fluorometric Determination of Beryllium

2017-3-17  A RAPID METHOD FOR FLUOROMETRIC DETERMINATION OF BERYLLIUM BY J. M. RILEY • • II • II • -It Report of lnveatigations 5282 UNITED STATES DEPARTMENT OF THE INTERIOR Fred A. Seaton, Secretary BUREAU OF MINES Marling J. Ankeny, Director Work on manuscript completed April 1956.

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Determination of Beryllium in Ores Fluorometric Method

2021-3-12  Determination of Beryllium in Ores Fluorometric Method. Mary H. Fletcher, Charles E. White, and ; Some observations on the use of 1,4-dihydroxyanthraquinone as a fluorometric reagent for traces of lithium. Analytical Chemistry of Beryllium. VIII. Fluorometric Determination of Micro Quantities of Beryllium with 8-Hydroxyquinaldine.

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Determination of Beryllium in Ores Fluorometric Method

A method is described for the accurate and precise determination of boron, beryllium and lithium in coal ash and geological materials by a point-to-plane high-voltage spark optical emission

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[Determination of beryllium in blood by fluorometric

[Determination of beryllium in blood by fluorometric analysis (author's transl)]. [Article in Japanese] Takata T, Hitosugi M, Kadowaki T, Inoue Y, Seki K. PMID: 691845 [PubMed indexed for MEDLINE] MeSH Terms. Beryllium/blood* Fluorometry/methods* Humans; Substances. Beryllium

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Improvements in the Fluorometric Determination of

2019-5-25  Fluorometric determination of submicrogram quantities of tin. Analytical Chemistry 1971, 43 Gas chromatographic determination of beryllium in biological materials and in air. Environmental Science & Technology 1969, 3 Graphite furnace atomic absorption spectrometry as a routine method for the quantification of beryllium in blood and serum.

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Determination of beryllium in drinking water by

METHOD. The fluorimetric method for the determination of beryllium is based on the formation of a complex compound between beryllium and morin in alkaline medium in the presence of masking agents followed by the measurement of fluorescence intensity of the formed complex compound using Fluorat-02 analyzer. The result appears on the PC-operated

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Fluorometric Determination of Ethylenediamine Using a

2017-3-8  A fluorometric method for the determination of en by using the beryllium(II) complex has been established. Ethylenediamine could be determined in 2×10 −7 –2×10 −5 mol dm −3 within a relative standard deviation of 3%.

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Standard Test Method for Determination of Beryllium in

5.1 Exposure to beryllium can cause a potentially fatal disease, and occupational exposure limits for beryllium in air and on surfaces have been established to reduce exposure risks to potentially affected workers (4, 5).Sampling and analytical methods for beryllium are needed in order to meet the challenges relating to exposure assessment and risk reduction.

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MONITOR FOR THE QUANTITATIVE DETERMINATION OF

@article{osti_4114381, title = {MONITOR FOR THE QUANTITATIVE DETERMINATION OF BERYLLIUM IN THE ATMOSPHERE}, author = {Webb, M S.W. and Webb, R J and Wildy, P C}, abstractNote = {Air was drawn through a triggered intermittent arc and the intensity of the beryllium doublet at 3130 A was monitered, together with the adjacent background; and the ratio of these intensities was recorded on a

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Fluorometric Determination of Ethylenediamine Using a

2017-3-8  A fluorometric method for the determination of en by using the beryllium(II) complex has been established. Ethylenediamine could be determined in 2×10 −7 –2×10 −5 mol dm −3 within a relative standard deviation of 3%.

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Selective determination of beryllium(II) ion at picomole

A highly sensitive and selective method for the determination of the Be(II) ion has been developed by the use of reversed-phase high-performance liquid chromatography (HPLC) with fluorometric detection using 2-(2′-hydroxyphenyl)-10-hydroxybenzo[h]quinoline (HPHBQ) as a precolumn (off-line) chelating reagent.

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Selective Determination of Beryllium(II) Ion at Picomole

A highly sensitive and selective method for the determination of the Be(II) ion has been developed by the use of reversed-phase high-performance liquid chromatography (HPLC) with fluorometric

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Studies on the Fluorometric Analysis. (VI) : Flurometric

2016-6-16  The interfering elements in the determination of aluminum by this method are Fe3+, Ga, Co, and vanadic acid. Also, the presence of a large amount of Cu, Ti, and Ni has a disturbing influence. Studies on the Fluorometric Analysis. (V) Determination of Gallium with 8-Hydroxyquinaldine

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Selective determination of beryllium(II) ion at picomole

2003-2-1  Selective determination of beryllium(II) ion at picomole per decimeter cubed levels by kinetic differentiation mode reversed-phase high-performance liquid chromatography with fluorometric detection using 2-(2'-hydroxyphenyl)-10-hydroxybenzo[H]quinoline as precolumn chelating reagent. Matsumiya H(1), Hoshino H.

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MONITOR FOR THE QUANTITATIVE DETERMINATION OF

@article{osti_4114381, title = {MONITOR FOR THE QUANTITATIVE DETERMINATION OF BERYLLIUM IN THE ATMOSPHERE}, author = {Webb, M S.W. and Webb, R J and Wildy, P C}, abstractNote = {Air was drawn through a triggered intermittent arc and the intensity of the beryllium doublet at 3130 A was monitered, together with the adjacent background; and the ratio of these intensities was recorded on a

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ASTM-D7202 Standard Test Method for Determination of

See Test Method D7458 for determination of beryllium in soil samples. 1.4 This test method includes a procedure for extraction (dissolution) of beryllium in weakly acidic medium (pH of 1 % aqueous ammonium bifluoride is 4.8), followed by field analysis of aliquots of the extract solution using a beryllium-specific-optically fluorescent dye.

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Standard Test Method for Determination of Beryllium in

1. Scope. 1.1 This test method is intended for use in the determination of beryllium by sampling workplace air and surface dust. 1.2 This test method assumes that air and surface samples are collected using appropriate and applicable ASTM International standard practices for sampling of

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FLUOROMETRIC DETERMINATION OF ACETYLSALICYLIC

2015-7-2  The Fluorometric Determination of Acetylsalicylic Acid in an Aspirin Tablet Introduction: Fluorescence is the emission of radiation from an atom or polyatomic species after the substance has been exposed to electromagnetic radiation. The incident radiation results in excitation of the substance.

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Development and validation of a fluorometric method

2012-12-10  the determination of hesperidin in plasma was 0.02–10.00 μg mL-1 with an LOD 0.005 g mLμ-1 and an LOQ of 0.015 μg mL-1. The good agreement between the two methods indicates the usability of the proposed fluorometric method for the simple, precise and accurate determination of hesperidin in cli-nical and quality control laboratories.

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Selective Determination of Beryllium(II) Ion at Picomole

A highly sensitive and selective method for the determination of the Be(II) ion has been developed by the use of reversed-phase high-performance liquid chromatography (HPLC) with fluorometric

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Spectrofluorimetric Determination of Beryllium by Mean

2016-6-6  Trace amounts of beryllium has been determined by spectrofluorimetric method that used morin as fluorimetric reagent. Beryllium gives a highly fluorescent complex with morin. The excitation wavelength of morin and Be-morin complex were 410 and 430. The fluorescence spectra of morin and Be-morin complex were overlaped in excitation wavelength of 430 nm. A method based on mean

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BERYLLIUM in Air 7704 by Field-Portable Fluorometry

2007-4-6  OTHER METHODS: Method 7300 (hot plate digestion and inductively coupled plasma atomic emission spectrometry) is an alternative (reference) procedure for the determination of elemental beryllium [3]. ASTM method D7202 is a similar proce-dure to detect elemental beryllium

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Ultra-trace determination of beryllium in occupational

A highly sensitive molecular fluorescence method for measuring ultra-trace levels of beryllium has been previously described. The method entails extraction of beryllium workplace samples by 1% ammonium bifluoride (NH(4)HF(2), aqueous), followed by fluorescence detection using hydroxybenzoquinoline sulfonate (HBQS).

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ASTM-D7202 Standard Test Method for Determination of

See Test Method D7458 for determination of beryllium in soil samples. 1.4 This test method includes a procedure for extraction (dissolution) of beryllium in weakly acidic medium (pH of 1 % aqueous ammonium bifluoride is 4.8), followed by field analysis of aliquots of the extract solution using a beryllium-specific-optically fluorescent dye.

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Development and validation of a fluorometric method

2012-12-10  the determination of hesperidin in plasma was 0.02–10.00 μg mL-1 with an LOD 0.005 g mLμ-1 and an LOQ of 0.015 μg mL-1. The good agreement between the two methods indicates the usability of the proposed fluorometric method for the simple, precise and accurate determination of hesperidin in cli-nical and quality control laboratories.

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Fluorometric Enzyme Assays Creative Enzymes

Fluorometric assays are widely used for the determination of the kinetic mechanism of enzyme reactions, and are also used to configure kinetic assays for high throughput screening. To be measured with a fluorescence-based assay the reaction needs to

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Principles of Assay Procedures DSM

these methods. Techniques also exist for simultaneous determination of all water-soluble vitamins by HPLC using UV/visible spectrophotometric detection. Vitamin C assays Vitamin C can be quantitatively analyzed by either titrimetric or fluorometric methods. The titrimetric method (Fig. 4) involves the measurement of decolorization of 2,6

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A rapid and sensitive fluorometric assay method for the

2010-12-23  A rapid, simple and sensitive fluorometric assay method for the determination of nitrilase activity is described. 3-Cyanopyridine was hydrolysed to nicotinic acid by Rhodococcus rhodochrous and the liberated NH 3 was allowed to react with buffered o-phthaldialdehyde-2-mercaptoethanol solution (pH 7.4) to form a fluorochrome.The fluorescence intensity was found to be stable after 20 min

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FLUOROMETRIC DETERMINATION OF ACETYLSALICYLIC

2015-7-2  The Fluorometric Determination of Acetylsalicylic Acid in an Aspirin Tablet Introduction: Fluorescence is the emission of radiation from an atom or polyatomic species after the substance has been exposed to electromagnetic radiation. The incident radiation results in excitation of the substance.

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